Lithium Hydroxide → HCID 67393125, compound

Participants

Reaction Conditions

Reaction Steps

Methyl 4-[(E)-2-(1-methyl-1H-pyrrol-2-yl)ethenyl]benzoate (40 mg, 0.166 mmol; see step (i) above) was suspended in a mixture of methanol (1 mL) and lithium hydroxide solution (16 mg of LiOH in water 2 mL). The reaction mixture was heated at 60° C. overnight with stirring. This solution was freeze-dried and the title compound used in the next step without further purification.

Provenance & Evidence