Thionyl Chloride → HCID 11310415, compound

Participants

Reaction Steps

3-Quinolinylmethanol (that prepared step (i) above) was dissolved in DCM (2 mL) and SOCl2 (5 mL) was added (dropwise initially) to the solution, which was then refluxed for 1 h. The DCM and excess SOCl2 were then removed under reduced pressure to yield the sub-title compound, which was employed directly in the next step without further purification.

Provenance & Evidence