Acetone → HCID 59003816, compound

HRID 907435Notes

Reaction equation

[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[C:4]([Cl:9])[CH:3]=1.[CH3:10][C:11]([CH3:13])=O>>[Cl:9][C:4]1[CH:3]=[C:2]([N:1]=[C:11]([CH3:13])[CH3:10])[CH:7]=[CH:6][C:5]=1[OH:8]

Participants

Reactant 2

HCID 180Acetone

HCID 775784-Amino-2-chlorophenol

Product 1

HCID 59003816HCID 59003816, compound

Procedure

4-amino-2-chloro-phenol Compound 13a was refluxed with acetone to provide 2-chloro-4-isopropylideneamino-phenol Compound 13b in quantitative yield. MS (ESI) m/z: 185 (M+H+).

Sources & evidence

ORD record: ord-fb13a86b4b474439ad39fa45c72ee4e8
Source dataset: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08013153B2

Reaction notes

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