HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → HCID 86611256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 58828852 | HCID 58828852 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86611256 | HCID 86611256 | — |
Reaction Steps
6-(isoquinolin-5-yl)-1-naphthoic acid (0.123 g, 0.4 mmol) was suspended in CH2Cl2 (15 mL) and oxallyl chloride was (0.036 mL, 0.4 mmol) was added followed by a drop of DMF. The resulting mixture was stirred at room temperature overnight and the solvent was evaporated to give a solid. The solid was dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017601B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-1b61ae75c8f94eb99daacc1196c64c57 |
| Source note | uspto-grants-2011_09 |