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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 908325Generated: November 2, 2026

Chloride → HCID 86611256, compound

https://huagongshe.com/reaction/908325

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorideHCID 312—
ReactantDimethylformamideHCID 6228—
ReactantHCID 58828852HCID 58828852—
SolventDichloromethaneHCID 6344—
ProductHCID 86611256HCID 86611256—

Reaction Steps

6-(isoquinolin-5-yl)-1-naphthoic acid (0.123 g, 0.4 mmol) was suspended in CH2Cl2 (15 mL) and oxallyl chloride was (0.036 mL, 0.4 mmol) was added followed by a drop of DMF. The resulting mixture was stirred at room temperature overnight and the solvent was evaporated to give a solid. The solid was dried under vacuum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08017601B2
Source datasetuspto-grants-2011_09
ORD IDord-1b61ae75c8f94eb99daacc1196c64c57
Source noteuspto-grants-2011_09