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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 908533Generated: October 30, 2026

Trifluoroacetic acid → HCID 59463765, compound

https://huagongshe.com/reaction/908533

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 59463762HCID 59463762—
SolventDichloromethaneHCID 6344—
ProductHCID 59463765HCID 5946376565%

Reaction Steps

TFA (2 ml) was added to a solution of compound 42 (100 mg, 0.18 mmol) in dichloromethane (4 ml) and the solution was stirred at room temperature. After 30 min the solvents were evaporated in vacuo and the afforded residue was purified by column chromatography on silica gel which gave the title compound (52 mg, 65%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08017620B2
Source datasetuspto-grants-2011_09
ORD IDord-6614962b560742cbb904a1d95279d8ee
Source noteuspto-grants-2011_09