Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 178514141 | HCID 178514141 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178508244 | HCID 178508244 | 75% |
Reaction Steps
A solution of the compound (0.20 g) obtained in Step 2 in N,N-dimethylformamide (7.0 ml) was stirred overnight under heating at 135° C. The reaction mixture was cooled to room temperature, and water (7.0 ml) was added under ice-cooling. The precipitated solid was collected by filtration, washed with water and dried to give the title compound (0.15 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08017612B2 |
|---|
| Source dataset | uspto-grants-2011_09 |
|---|
| ORD ID | ord-e13312c5756144e7accf0d7320a633ae |
|---|
| Source note | uspto-grants-2011_09 |
|---|
