HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 15758917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 3-(4-Methylphenyl)propan-1-ol | HCID 221893 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15758917 | HCID 15758917 | — |
Reaction Steps
Following the procedure described in example 1§B, but starting from 3-(4-methylphenyl)propan-1-ol (6.02 g), triethylamine (2.9 mL), methanesulfonyl chloride (3.67 mL) and dichloromethane (39 mL), affords 3-(4-methylphenyl)propan-1-ol mesylate (3.4 g) used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017646B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-d74b549362eb489c93859f0f913ceed9 |
| Source note | uspto-grants-2011_09 |