HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 3-(Naphthalen-2-yl)propyl methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2-Naphthalenepropanol | HCID 11206232 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-(Naphthalen-2-yl)propyl methanesulfonate | HCID 11161385 | — |
Reaction Steps
Following the procedure described in example 1§B, but starting from 3-(2-naphtyl)propan-1-ol (11.7 mmol), triethylamine (2.5 mL), methanesulfonyl chloride (1.7 mL) and dichloromethane (50 mL), affords 1.7 g of 3-(2-naphtyl)propan-1-ol mesylate used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017646B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-1213e379f0bf45dab0f2e217c0f3cb93 |
| Source note | uspto-grants-2011_09 |