HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 86621824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Oxalate | HCID 71081 | — |
| Reactant | 3'-Hydroxyisosafrole | HCID 5869753 | — |
| Reactant | 1-(3-chloropropyl)pyrrolidine Hydrochloride | HCID 11571916 | — |
| Product | HCID 86621824 | HCID 86621824 | — |
Reaction Steps
Following the procedure described in example 2, but starting from trans-5-(3-hydroxyprop-1-en-1-yl)benzodioxolane (400 mg), potassium hydroxide (283 mg, 85% wt) and 1-(3-chloropropyl)pyrrolidine, hydrochloride (376 mg) in dimethylsufoxide (5 mL) affords 90 mg of trans-1-{3-[3-(benzodioxol-5-yl)allyloxy]-propyl}pyrrolidine, oxalate as a white solid melting at 109-111° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017646B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-f1e4951bd5f64f0b9ede78f476b9043a |
| Source note | uspto-grants-2011_09 |