HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 11568096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 11568097 | HCID 11568097 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 11568096 | HCID 11568096 | 69% |
Reaction Steps
2-(4-Dimethylamino-4-phenylcyclohexylidene)-N-(4-phenyl-butyl)acetamide (292 mg, 0.747 mmol) was dissolved in ethyl methyl ketone (5 ml), and chlorotrimethylsilane (0.14 ml, 1.12 mmol) was added. After 1.5 h the hydrochloride was isolated as a colourless solid in a yield of 69% (221 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017630B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-effb245f9533461f9b1e04a13fe127ed |
| Source note | uspto-grants-2011_09 |