HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 11711633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 11711634 | HCID 11711634 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 11711633 | HCID 11711633 | 30% |
Reaction Steps
2-(4-Dimethylamino-4-phenylcyclohexyl)-N-(4-phenylbutyl)acetamide (194 mg, 0.49 mmol) was dissolved in ethyl methyl ketone, and chlorotrimethylsilane (0.093 ml, 0.74 mmol) was added. After 1.5 h it was possible to filter off the product with suction as a colourless, hygroscopic solid in a yield of 30% (63 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017630B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-5e72816c9f124060bf723d16bbb79b80 |
| Source note | uspto-grants-2011_09 |