Hydrochloric Acid → HCID 86594427, compound

HRID 909216Notes

Reaction equation

HRID 909216 reaction equation
[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH:13]C(OC(C)(C)C)=O)[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8].[ClH:22]>>[ClH:22].[ClH:22].[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH2:13])[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 86594426HCID 86594426, compound

Product 1

HCID 86594427HCID 86594427, compound

Procedure

(S)-2-tert-Butoxycarbonylamino-4-[(2-methoxyethyl)-methylamino]-butyric acid methyl ester (0.086 g, 0.28 mmol) was treated with HCl (1 mL of 4M in dioxane) and sonicated. The mixture was concentrated and dried under high vacuum to provide the product.

Workup

  1. customsonicated
  2. concentrationThe mixture was concentrated
  3. customdried under high vacuum
  4. customto provide the product

Sources & evidence

ORD record
ord-c6b75837598e49c4b14507a8a40a53dd
Source dataset
uspto-grants-2011_09
Patent number
US08017641B2

Reaction notes

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