HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 44417462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | (2-hydroxy-5-methylphenyl)(1-phenyl-1H-pyrazol-4-yl)methanone | HCID 688698 | — |
| Product | HCID 44417462 | HCID 44417462 | — |
Reaction Steps
Prepared from (2-hydroxy-5-methylphenyl)-(1-phenyl-1H-pyrazol-4-yl)-methanone and ethyl bromoacetate according to GP2 and GP3: LC/MS (an 10p8): Rt 3.08 min, m/z 356.6 [M+1]+; 1H NMR (CDCl3): δ2.37 (s, 3H), 4.78 (s, 2H), 6.97 (d, J=9.0 Hz, 1H), 7.33-7.51 (m, 5H), 7.73 (d, J=6 Hz, 2H), 8.16 (s, 1H), 8.51 (s, 1H), 11.21 (br s, 1H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022063B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-0da7167259434c26ab57705d9f806039 |
| Source note | uspto-grants-2011_09 |