HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67241484, compound → HCID 57658835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67241484 | HCID 67241484 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57658835 | HCID 57658835 | — |
Reaction Steps
A mixture of ethyl 4-nitro-2-(phenyl-1H-pyrazole-4-carbonyl)phenoxyacetate (190 mg, 0.48 mmol) and 10% Pd/C (100 mg) in MeOH (50 mL) was stirred under an atmosphere of hydrogen of 12 h, then filtered through a pad of celite and concentrated, and the product was hydrolyzed according to GP3 to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022063B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-41dfbd570a3e4f4487bac6620edbec83 |
| Source note | uspto-grants-2011_09 |