Phenacyl bromide → HCID 57658770, compound

HRID 910045Notes

Reaction equation

HRID 910045 reaction equation
C([O:3][C:4](=[O:17])[CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([Br:13])=[CH:9][C:8]=1[C:14](=[O:16])[NH2:15])C.Br[CH2:19][C:20]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)=O>>[Br:13][C:10]1[CH:11]=[CH:12][C:7]([O:6][CH2:5][C:4]([OH:3])=[O:17])=[C:8]([C:14]2[O:16][CH:19]=[C:20]([C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[N:15]=2)[CH:9]=1

Participants

3

Reactant 2

HCID 6259Phenacyl bromideHCID 57658729Ethyl 2-[2-(aminocarbonyl)-4-bromophenoxy]acetate

Product 1

HCID 57658770HCID 57658770, compound

Procedure

Title compound was prepared from (4-bromo-2-carbamoylphenoxy)acetic acid ethyl ester and 2-bromoacetophenone according to GP7: LC/MS (an 10p8) Rt 2.32 min, m/z 374/376 [M+H]+.

Sources & evidence

ORD record
ord-0578241f77fc43f783a40403f8cc1a3c
Source dataset
uspto-grants-2011_09
Patent number
US08022063B2

Reaction notes

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