Water → HCID 67405072, compound

Participants

Reaction Steps

2-Amino-5-iodopyridine (1.0 g) and 2-bromo-4′-cyanoacetophenone (1.02 g) were dissolved in ethanol (30 mL), and sodium hydrogencarbonate (382 mg) was added to the solution, followed by refluxing for 16 hours. Water (10 mL) was added to the reaction mixture, and the mixture was left to cool. The precipitated matter was recovered through filtration and dried, to thereby yield the title compound (1.27 g).

Provenance & Evidence