HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 16735616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Tosylmethyl isocyanide | HCID 161915 | — |
| Reactant | HCID 16738347 | HCID 16738347 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16735616 | HCID 16735616 | 45.9% |
Reaction Steps
4-(6-Iodoimidazo[1,2-a]pyridin-2-yl)benzaldehyde (647 mg) and p-toluenesulfonylmethyl isocyanide (454 mg) were dissolved in methanol (10 mL), and potassium carbonate (321 mg) was added to the solution at room temperature, followed by refluxing for 13 hours. The precipitated product was recovered through filtration and dried, to thereby yield the title compound (330 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022075B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-566a10d1a880433c8a2abb72a75aa68c |
| Source note | uspto-grants-2011_09 |