Hydrochloric Acid → HCID 16735147, compound

Participants

Reaction Conditions

Reaction Steps

4-(6-Iodoimidazo[1,2-a]pyridin-2-yl)benzonitrile (345 mg) and thioacetamide (150 mg) were added to a saturated solution (5 mL) of hydrogen chloride in dimethylformamide. The mixture was heated at 80° C. for 4 hours, and the solvent was evaporated. Saturated sodium hydrogencarbonate was added to the residue, followed by recovering the solid through filtration and drying, to thereby yield the title compound (269 mg).

Provenance & Evidence