HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178513272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 67405072 | HCID 67405072 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178513272 | HCID 178513272 | 73.8% |
Reaction Steps
Hydroxylamine hydrochloride (208 mg) and potassium carbonate (415 mg) were added to a solution (10 mL) of 4-(6-iodoimidazo[1,2-a]pyridin-2-yl)benzonitrile (345 mg) in methanol, followed by refluxing for 14 hours. The mixture was left to cool, and the formed crystals were recovered through filtration. The crystals were washed with water and dried, to thereby yield the title compound (279 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022075B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-51f1098e9d094c048df072de84218fe9 |
| Source note | uspto-grants-2011_09 |