Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 910217Generated: October 31, 2026

Potassium Carbonate → HCID 178513272, compound

https://huagongshe.com/reaction/910217

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantHCID 67405072HCID 67405072—
SolventMethanolHCID 887—
ProductHCID 178513272HCID 17851327273.8%

Reaction Steps

Hydroxylamine hydrochloride (208 mg) and potassium carbonate (415 mg) were added to a solution (10 mL) of 4-(6-iodoimidazo[1,2-a]pyridin-2-yl)benzonitrile (345 mg) in methanol, followed by refluxing for 14 hours. The mixture was left to cool, and the formed crystals were recovered through filtration. The crystals were washed with water and dried, to thereby yield the title compound (279 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08022075B2
Source datasetuspto-grants-2011_09
ORD IDord-51f1098e9d094c048df072de84218fe9
Source noteuspto-grants-2011_09