HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinamine, 5-iodo- → HCID 67404368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinamine, 5-iodo- | HCID 88579 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 86761410 | HCID 86761410 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67404368 | HCID 67404368 | — |
Reaction Steps
Subsequently, 2-amino-5-iodopyridine (478 mg) and tert-butyl 4-[4-(2-bromoacetyl)phenyl]-1H-1-pyrazolecarboxylate mg) were dissolved in ethanol (20 mL), and sodium hydrogencarbonate (183 mg) was added to the solution, followed by refluxing for 16 hours. The precipitated matter was recovered through filtration and dried, to thereby yield the title compound (535 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022075B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-e5d440f8ce4e4ff68bbc7347f28c4e14 |
| Source note | uspto-grants-2011_09 |