HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → Ethyl (diethoxyphosphoryl)ethoxyacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | Ethyl 2-(2-chloroethoxy)acetate | HCID 10964894 | — |
| Product | Ethyl (diethoxyphosphoryl)ethoxyacetate | HCID 15729465 | 100% |
Reaction Steps
36.3 g (218 mmol) of ethyl chloroethoxyacetate and 37.4 ml (218 mmol) of triethyl phosphite are heated at 50° C. for 3 hours. The reaction medium is evaporated to dryness under vacuum. 57 g (100%) of crude ethyl (d iethoxyphosphoryl)ethoxyacetate are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022079B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-830901ebf3824f7f9910b2e3512eaff5 |
| Source note | uspto-grants-2011_09 |