HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 57613219, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 67388409 | HCID 67388409 | — |
| Product | HCID 57613219 | HCID 57613219 | — |
Reaction Steps
A solution of 4-(6-thiophen-2-yl-pyrimidin-4-yl)-piperazine-1-carboxylic acid tert-butyl ester (30 mg, 0.08 mmol) in 1:1 TFA/CH2Cl2 (3 mL) was stirred for 2 h, and then was concentrated to yield the title compound, as its corresponding TFA salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022209B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-645eeda479f344969a8010b97f9d820d |
| Source note | uspto-grants-2011_09 |