HRID910744

反应详情

EQUATION

反应方程式

HRID 910744 的结构方程式

PROCEDURE

实验过程

Alkylation of 3-bromo-5-ethoxy-4-hydroxy benzaldehyde (2 g) with 3-bromomethyl-benzoic acid methyl ester (2.06 g) was performed according to the method described in example 1a. The residue was chromatographed on silica gel in heptane/ethyl acetate=7/3 (v/v) as eluent. Yield: 2.42 g. MS-ESI: [M+H]+=393/395

WORKUP

后处理

  1. customThe residue was chromatographed on silica gel in heptane/ethyl acetate=7/3 (v/v) as eluent