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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 910800Generated: October 29, 2026

HCID 67061780, compound → HCID 86651707, compound

https://huagongshe.com/reaction/910800

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67061780HCID 67061780—
SolventEthylacetate heptaneHCID 21899848—
ProductHCID 86651707HCID 86651707—

Reaction Steps

The title compound is prepared according to general procedure F starting from 1.0 mmol of [(2S,4R,5R)-4-[4-((S)-3-methoxy-2-methyl-propoxymethyl)-phenyl]-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-1-(toluene-4-sulfonyl)-piperidin-2-yl]-methanol. Rf=0.45 (EtOAc/heptane 2:1); Rt=5.52 (gradient I).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08022068B2
Source datasetuspto-grants-2011_09
ORD IDord-2747c0d7e4944d8fb6d857ff2d6a8375
Source noteuspto-grants-2011_09