HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67061780, compound → HCID 86651707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67061780 | HCID 67061780 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 86651707 | HCID 86651707 | — |
Reaction Steps
The title compound is prepared according to general procedure F starting from 1.0 mmol of [(2S,4R,5R)-4-[4-((S)-3-methoxy-2-methyl-propoxymethyl)-phenyl]-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-1-(toluene-4-sulfonyl)-piperidin-2-yl]-methanol. Rf=0.45 (EtOAc/heptane 2:1); Rt=5.52 (gradient I).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022068B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-2747c0d7e4944d8fb6d857ff2d6a8375 |
| Source note | uspto-grants-2011_09 |