Sodium borohydride → HCID 67392158, compound

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Reaction Steps

The product from step (i) (2.0 g) was dissolved in dry ethanol (20 ml) then sodium borohydride (0.15 g) added. The mixture was stirred at RT overnight then evaporated under reduced pressure to give a white solid. The solid was partitioned between 2M hydrochloric acid and ethylacetate, the organics were dried and evaporated under reduced pressure, yield 0.70 g.

Provenance & Evidence