Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 67392158 | HCID 67392158 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86620100 | HCID 86620100 | — |
Reaction Steps
Triethylamine (0.33 ml) followed by methanesulphonyl chloride (0.185 ml) were added to a solution of the product from step (ii) (0.7 g) in DCM (20 ml) at −20° C. The mixture was stirred at 0° C. for 1 h, then diluted with dichloromethane, washed with water, dried and evaporated under reduced pressure, yield 0.97 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08022248B2 |
|---|
| Source dataset | uspto-grants-2011_09 |
|---|
| ORD ID | ord-12c96d1b8b584a0fb70b46002f63775e |
|---|
| Source note | uspto-grants-2011_09 |
|---|
