反应详情

Sodium borohydride (0.223 g) was added to a solution of the product from step (ii) (1.07 g) in dry ethanol (30 ml) and the mixture was stirred at RT overnight. The mixture was partitioned between 2M hydrochloric acid/ethyl acetate, the organics separated, dried and evaporated under reduced pressure, yield 1.08 g.

1. customThe mixture was partitioned between 2M hydrochloric acid/ethyl acetate
2. customthe organics separated, dried
3. customevaporated under reduced pressure, yield 1.08 g