Potassium Carbonate → HCID 178513351, compound

Participants

Reaction Steps

The subtitle compound was prepared using the product from example 29 step i) (0.60 g) which was dissolved in ethanol (20 ml) and treated with hydroxylamine hydrochloride (0.30 g) followed by potassium carbonate (0.60 g). The mixture was heated at 90 C for 2 hours, cooled and the solid filtered off. The filtrate was concentrated under reduced pressure to give a red oil. Yield 0.94 g.

Provenance & Evidence