Methanol → HCID 11653774, compound

Participants

Reaction Steps

A mixture of the product from step (ii) (0.5 g), methanol (5 ml), water (4 ml) and 2M NaOH (2 ml) were stirred at room temperature for 4 h then partitioned between ethylacetate/2 M HCl. The organics were separated, washed with water, dried and evaporated under reduced pressure. The residue was triturated with diethylether/isohexane and filtered, yield 0.1 g.

Provenance & Evidence