HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vinyl Acetate → HCID 19809220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vinyl Acetate | HCID 7904 | — |
| Reactant | 4-Bromobutyric acid | HCID 75809 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Product | HCID 19809220 | HCID 19809220 | — |
Reaction Steps
To 4-bromobutyric acid (1.0 g, 6.0 mmol) in vinyl acetate (54 mL) add with stirring palladium(II) acetate (188 mg, 0.84 mmol) and continue stirring overnight at ambient temperature. Filter and concentrate in vacuo to provide the crude desired intermediate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022062B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-c01875a808384d229c67590cfc2f0787 |
| Source note | uspto-grants-2011_09 |