HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Chloromethyl)-6-methoxypyridine--hydrogen chloride (1/1) → HCID 66706891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Chloromethyl)-6-methoxypyridine--hydrogen chloride (1/1) | HCID 54593011 | — |
| Reactant | 3-tert-butoxycarbonyl-7-chloro-6-dimethylaminocarbonylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine | HCID 57655979 | — |
| Product | HCID 66706891 | HCID 66706891 | — |
Reaction Steps
Use a method similar to the Example 330, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 2-chloromethyl-6-methoxypyridine hydrochloride to give, after deprotection by a method similar to the General Procedure 14, the title compound as a white solid (120 mg). MS (APCI+) m/z: 335 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022062B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-f973790b05244d68ab8acd540245f2a9 |
| Source note | uspto-grants-2011_09 |