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HRID911521

反应详情

EQUATION

反应方程式

HRID 911521 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)Oc1ccc(CCl)cc1
HCID148312

Phenol, 4-(chloromethyl)-, acetate

C9H9ClO2

结构：CN(C)C(=O)Sc1c(Cl)ccc2c1CCN(C(=O)OC(C)(C)C)CC2
HCID57655979

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)Oc1ccc(CSc2c(Cl)ccc3c2CCN(C(=O)OC(C)(C)C)CC3)cc1
HCID57656056

未命名化合物

PROCEDURE

实验过程

Use a method similar to the Preparation 177, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 4-(chloromethyl)phenyl acetate to give 6-(4-acetoxybenzylthio)-3-tert-butoxycarbonyl-7-chloro-2,3,4,5-tetrahydro-1H-benzo[d]azepine as a white solid.

WORKUP

后处理

  1. customsimilar to the Preparation 177