HRID911740

反应详情

EQUATION

反应方程式

HRID 911740 的结构方程式

PROCEDURE

实验过程

Example 647 may be prepared essentially as described in Example 646 using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 2,2-difluoro-2-pyridin-2-yl-ethyl trifluoromethanesulfonate (prepared by following the procedure described in J. Med. Chem. 2003, 46, 461-473) (66% yield, MS (ES+) m/z 355 (M+H)+).

WORKUP

后处理

  1. customExample 647 may be prepared essentially
  2. customprepared