Trifluoroacetic acid → HCID 24888238, compound

Participants

Reaction Steps

4-(3-t-Butoxy-phenyl)-2-morpholin-4-yl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-carbaldehyde (5 mg) obtained from Example 1-C-07 as a byproduct was treated with trifluoroacetic acid (1 ml), and the solvent was distilled off, which was subsequently diluted with water (1 ml), and extracted with dichloromethane (3 ml×3), followed by concentration under reduced pressure, to obtain a colorless powder (2 mg, 47%).

Provenance & Evidence