HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 723128, compound → HCID 16795691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 723128 | HCID 723128 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16795691 | HCID 16795691 | — |
Reaction Steps
To methanol solution (5 ml) of (4-ethyl-piperazin-1-yl)-(3-nitro-phenyl)-methanone (365.3 mg) obtained in Step A, palladium black was added, followed by stirring at room temperature for 14 hours under a hydrogen gas atmosphere. This was filtered through Celite, and subsequently the solvent was distilled off under reduced pressure, to obtain the desired compound as a crude product (241.8 mg, 51%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022205B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-60522f35b9f34244bfb4ca6e63e29c0b |
| Source note | uspto-grants-2011_09 |