HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoic Acid → (4-Methylpiperazin-1-yl)(4-nitrophenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoic Acid | HCID 6108 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Product | (4-Methylpiperazin-1-yl)(4-nitrophenyl)methanone | HCID 716396 | — |
Reaction Steps
Using 4-nitro-benzoic acid (1 g) instead of 3-nitro-benzoic acid, and 1-methyl-piperazine (797 μl) instead of 1-ethyl-piperazine, in the same manner as Step A in Example 1-D-101, the desired compound was obtained as a crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022205B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-e3c7ed43b1a44dff9dd04794aa9cdd7e |
| Source note | uspto-grants-2011_09 |