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HRID912438

反应详情

EQUATION

反应方程式

HRID 912438 的结构方程式

REACTANTS

反应物

2
结构：CI
HCID6328

Methyl iodide

CH3I

结构：CC(C)(C)OC(=O)N[C@H]1CCCNC1=O
HCID124787

3-tert-Butyloxycarbonylamino-2-piperidone

C10H18N2O3

PRODUCTS

生成物

1
结构：CN1CCC[C@H](NC(=O)OC(C)(C)C)C1=O
HCID57736564

未命名化合物

PROCEDURE

实验过程

(S)-tert-butyl 1-methyl-2-oxopiperidin-3-ylcarbamate was prepared from (S)-tert-butyl 2-oxopiperidin-3-ylcarbamate (Example 7) and methyl iodide according to the general procedure of Example 9. The crude product was purified by column chromatography, eluting with 100% ethyl acetate, to provide compound (2c) in 31% yield.

WORKUP

后处理

  1. customThe crude product was purified by column chromatography
  2. washeluting with 100% ethyl acetate