Formic Acid → HCID 16755779, compound

Participants

Reaction Steps

The title compound was prepared in accordance with the general method described in Example 1(d), using 5,6-diamino-1-(pyridin-4-ylmethyl)-2-thioxo-2,3-dihydro-1H-pyrimidin-4-one (0.25 g, 1.0 mmol, obtained from Example 3(b)), with the exception that 20 minutes of reaction time in formic acid was used, followed by a reaction time of 45 minutes in sodium hydroxide (10% aq.). The title compound was obtained (0.033, 13%) as a solid.

Provenance & Evidence