Sodium Dithionite → HCID 86631136, compound

Participants

Reaction Steps

The title compound was prepared in accordance with the general method described in Example 12(c) by using 6-amino-1-[(4-methyl-1,2,5-oxadiazol-3-yl)methyl]-2-thioxo-2,3-dihydropyrimidin-4(1H)-one (0.44 g, 1.8 mmol, obtained from Example 16(b)), sodium nitrite (0.14 g, 2.0 mmol) and sodium dithionite (0.64 g, 3.7 mmol) which gave the title compound (0.41 g, 88% yield).

Provenance & Evidence