HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methacrylate → Hydroxyethylimidazole Methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Phenothiazine | HCID 7108 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | 2-(1H-imidazol-2-yl)ethan-1-ol | HCID 15016080 | — |
| Product | Hydroxyethylimidazole Methacrylate | HCID 67198382 | — |
Reaction Steps
At a temperature of 65° C., methyl methacrylate (MMA) and hydroxyethylimidazole (HEI) in a molar ratio of 5:1 were heated in the presence of 50 ppm pf phenothiazine, 500 ppm of hydroquinone monomethyl ether and 1.25 mol % of a catalyst (based on hydroxyethylimidazole) for 5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026374B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-696a6f25c1e24b8d82b6cda02159c28b |
| Source note | uspto-grants-2011_09 |