Fluorine → Acrylic acid ethyl acrylate
Reaction equation
[Na].[C:2]([C:10]([O:16][CH2:17][CH2:18][O:19][C:20]1C=CC=[CH:22][CH:21]=1)(S([O-])(=O)=O)C)(CC(C)(C)C)(C)[CH3:3].[Na+].S1(=[O:36])C2C=CC=CC=2C=N1.FF.[K]>>[C:20]([OH:36])(=[O:19])[CH:21]=[CH2:22].[C:10]([O:16][CH2:17][CH3:18])(=[O:36])[CH:2]=[CH2:3]Participants
Procedure
A coating solution for protective layer on the back side was prepared by mixing 50 g of gelatin, 0.2 g of sodium polystyrenesulfonate, 2.4 g of N,N-ethylenebis(vinylsulfonacetamide), 1 g of sodium tert-octylphenoxyethoxyethanesulfonate, 30 mg of benzisothiazolinone, 37 mg of a fluorine-containing surfactant (F-1: potassium salt of N-perfluorooctylsulfonyl-N-propylalanine), 150 mg of a fluorine-containing surfactant (F-2: polyethylene glycol mono(N-perfluorooctylsulfonyl-N-propyl-2-aminoethyl) ether [average polymerization degree of ethylene oxide: 15]), 64 mg of a fluorine-containing surfactant (F-3), 32 mg of a fluorine-containing surfactant (F-4), 10 mg of a fluorine-containing surfactant (F-7), 5 mg of a fluorine-containing surfactant (F-8), 8.8 g of acrylic acid/ethyl acrylate copolymer (copolymerization ratio: 5/95 by weight), 0.6 g of Aerosol-OT (produced by American Cyanamid Co.), a liquid paraffin emulsion containing 1.8 g of liquid paraffin and 950 ml of water in a vessel kept at 40° C.
Workup
- customA coating solution for protective layer on the back side was prepared
- additioncontaining
Sources & evidence
- ORD record
- ord-6dfdb4ffa6624d25b5b5f1e73b8e686c
- Source dataset
- uspto-grants-2007_09
- Patent number
- US07264919B2
Reaction notes
Loading…