HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → HCID 10636022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | Benzenamine, 4-fluoro-N-(1-methylethyl)- | HCID 154403 | — |
| Reactant | 2-bromo-N-isopropyl-N-phenyl-acetamide | HCID 15216001 | — |
| Product | HCID 10636022 | HCID 10636022 | — |
Reaction Steps
Following the procedure described for Preparation 1(A); (4-fluoro-phenyl)-isopropyl-amine (13.70 g, 89.54 mmol) was alkylated with bromoacetyl bromide (7.78 mL, 89.54 mmol) to provide 15.02 g of 2-bromo-N-(4-fluoro-phenyl)-N-isopropyl-acetamide as an oil. 1H NMR (CD2Cl2) δ 7.14-7.23 (m, 4H), 4.90 (m, 1H), 3.53 (s, 2H), 1.05 (d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265104B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-2896178e4d89489f8c5342292e8c9f76 |
| Source note | uspto-grants-2007_09 |