HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17639086, compound → 3-amino-N-[2-(dimethylamino)ethyl]benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17639086 | HCID 17639086 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-amino-N-[2-(dimethylamino)ethyl]benzenesulfonamide | HCID 16790646 | 99.7% |
Reaction Steps
A solution of 3 (0.8 g) in ethanol (10 mL) was subjected to catalytic hydrogenation (10% Pd/C, Degussa, 0.8 g, 3 drops of AcOH, 1 atm.) overnight. To work up, the solids were filtered the filtrate was dried under vacuum to afford 4 as a solid (0.71 g) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265122B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-1a6e05943ec14adda9c6cee38578a3db |
| Source note | uspto-grants-2007_09 |