HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 27055575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Ethyl (3,4-dihydro-1H-isoquinolin-2-yl)acetate | HCID 2839036 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 27055575 | HCID 27055575 | 100% |
Reaction Steps
A solution of 90 (2.0 g, 9.12 mmol) and hydrazine (5.1 g, 91 mmol) in ethanol (30 mL) was heated at reflux overnight. The mixture was concentrated under reduced pressure to give 91 (1.87 g ˜100%) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265122B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-62c165ed74a74b769d7b88b2dc611239 |
| Source note | uspto-grants-2007_09 |