HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 69280242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | (6-Hydroxy-indol-1-yl)-acetic acid ethyl ester | HCID 68821422 | — |
| Reactant | HCID 69280234 | HCID 69280234 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 69280242 | HCID 69280242 | — |
Reaction Steps
In analogy to the procedure described for example 1 e], (6-hydroxy-indol-1-yl)-acetic acid ethyl ester was reacted with 5-chloromethyl-3-(4-chloro-phenyl)-1,4-dimethyl-1H-pyrazole in the presence of cesium carbonate and potassium iodide in acetone to give {6-[5-(4-chloro-phenyl)-2,4-dimethyl-2H-pyrazol-3-ylmethoxy]-indol-1-yl}-acetic acid ethyl ester as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265149B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-527ea52061564a5d8683ad2fd67d3a0d |
| Source note | uspto-grants-2007_09 |