HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 5-iodomethyl-1-methyl-3-(4-trifluoromethyl-phenyl)-1H-pyrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 5-chloromethyl-1-methyl-3-(4-trifluoromethyl-phenyl)-1H-pyrazole | HCID 21082224 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 5-iodomethyl-1-methyl-3-(4-trifluoromethyl-phenyl)-1H-pyrazole | HCID 69282812 | — |
Reaction Steps
In analogy to the procedure described in example 20 a], 5-chloromethyl-1-methyl-3-(4-trifluoromethyl-phenyl)-1H-pyrazole (example 9 a]) was treated with sodium iodide in acetone to obtain 5-iodomethyl-1-methyl-3-(4-trifluoromethyl-phenyl)-1H-pyrazole as yellow solid which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265149B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-6bf43f8f2469435dbe68adff14dfc595 |
| Source note | uspto-grants-2007_09 |