HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzoic acid → 2-Methoxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzoic acid | HCID 11370 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2-Methoxybenzoyl chloride | HCID 88969 | — |
Reaction Steps
A 1 ml (13.7 mmol) thionyl chloride solution of 136 mg (0.89 mmol) of o-anisic acid was heated under reflux for 2 hours. Then, the excess thionyl chloride was distilled off under reduced pressure to obtain o-anisic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268128B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-7603166fbe3c4febb991b172426d6256 |
| Source note | uspto-grants-2007_09 |