Tetrahydrofuran → HCID 136342085, compound

Participants

Reaction Conditions

Reaction Steps

A 2 ml tetrahydrofuran suspension of 100 mg (0.23 mmol) of the compound obtained in Example 31 was heated to 50° C. to form a solution. To this solution, 68 μl (0.27 mmol) of a 4M dioxane hydrochloride solution was added. Then, the reaction mixture was brought to room temperature, and ether was added. Precipitated solids were collected by filtration to obtain 96 mg (88%) of the captioned compound.

Provenance & Evidence