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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 915928Generated: October 30, 2026

HCID 136005913, compound → HCID 136005835, compound

https://huagongshe.com/reaction/915928

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 136005913HCID 136005913—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 136005835HCID 13600583599.5%

Reaction Steps

To a 50 ml methanol/50 ml tetrahydrofuran mixed solution of 1.16 g (2.61 mmol) of the compound obtained in Example 35, 300 mg of 5% palladium carbon was added. The mixture was stirred for 3 hours at room temperature at atmospheric pressure in an atmosphere of hydrogen. Then, the catalyst was removed by filtration to obtain 0.92 g (99%) of the captioned compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07268128B2
Source datasetuspto-grants-2007_09
ORD IDord-a6fc4f7137bd497fb0626445a1f98f79
Source noteuspto-grants-2007_09