HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136005913, compound → HCID 136005835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136005913 | HCID 136005913 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 136005835 | HCID 136005835 | 99.5% |
Reaction Steps
To a 50 ml methanol/50 ml tetrahydrofuran mixed solution of 1.16 g (2.61 mmol) of the compound obtained in Example 35, 300 mg of 5% palladium carbon was added. The mixture was stirred for 3 hours at room temperature at atmospheric pressure in an atmosphere of hydrogen. Then, the catalyst was removed by filtration to obtain 0.92 g (99%) of the captioned compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268128B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-a6fc4f7137bd497fb0626445a1f98f79 |
| Source note | uspto-grants-2007_09 |