HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 136338917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 136005929 | HCID 136005929 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 136338917 | HCID 136338917 | 77.3% |
Reaction Steps
A 1.15 ml ethanol suspended solution of 115 mg (0.255 mmol) of the compound obtained in Example 61 was heated to 60° C. To the system, 17.4 μl (0.267 mmol) of methanesulfonic acid was added, and the temperature of the mixture was gradually lowered to room temperature. Precipitated solids were collected by filtration to obtain 108 mg (77%) of the captioned compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268128B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-63cb18b581f24be99881c4bdb49ff0eb |
| Source note | uspto-grants-2007_09 |